EQUIPMENT CAPABILITIES AND SCALE (ORGANIC DIVISION)
Kilo Lab Scale – Glassware up to 72 L scale – Distillation support up to 50L scale
• Short path – Bench Strip – Rotary Evaporators • Long path – 18" to 48" packed columns – Stainless, Hastelloy, Ceramic packing
Pilot Scale – 10 gal – 100 gal glass lined steel
– 10 gal – 200 gal Stainless – Distillation Support • Rotary Evaporator • 30 gal – 50 gal glass lined steel distillation pots
– 4' to 12' columns – Glass & stainless packing Plant Scale – 350-500 gal Hastelloy – 100-1000 gal Glass – 200-1000 gal Stainless – Distillation support • Short path – 50 gal-500 gal glass lined • Long path/Fractional – 4' to 16' column – Stainless, Hastelloy, Glass packing
– Solids Handling • Hastelloy and Stainless centrifugation
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Plant Scale Supports – Vacuum capabilities to < 10 Torr
– Pressure handled to < 100 psi
– Reaction conditions controlled from -40o +140o
C
– Distillation conditions controlled from 20o
C to 250o C C to
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– Scrubbing supports for acid/base, ammonia and sulfide
– Nitrogen used as inerting atmosphere